####################### Meta Data Part ############################# Column Name Data Type Description Label Validation Text Unit 1 EXPEDITION Numeric expedition code expedition code (Int. 1 - 99999), required key field # 2 REQUEST Text request identifier, automatically generated # # 3 REQUEST_PART Text # request part ( A-Z), required key field # 4 REQUEST_TYPE Text type of sample request request type (max. 10 chars), required, valid request type # 5 REQUEST_DATE Date date request was entered request date (Date UTC), required field, valid date # 6 SCIENTIST_1 Integer identifier of first related scientist 1. scientist, required field, valid date # 7 SCIENTIST_2 Integer identifier of first related scientist # # 8 SCIENTIST_3 Integer identifier of first related scientist # # 9 PURPOSE Memo sample purpose # # 10 REMARKS Text optional additional remarks # # 11 APPROVAL_DATE Date date request was approved approval date (Date UTC), required field, valid date # 12 COMPLETION_DATE Date date request was completed completion date (Date UTC), required field, valid date # ####################### Data Part ############################# EXPEDITION REQUEST REQUEST_PART REQUEST_TYPE REQUEST_DATE SCIENTIST_1 SCIENTIST_2 SCIENTIST_3 PURPOSE REMARKS APPROVAL_DATE COMPLETION_DATE 5052 DFDP0000 A ShipShore 22-Nov-2011 12:00 Virginia Toy David Prior General petrological and microstructural characterisation; some focus on pseudotachylytes, fluid-related microscopic deformation eatures, etc impregnate with epoxy if friable; do not heat 5052 DFDP0001 A ShipShore 09-Nov-2011 12:00 Carolyn Boulton 48 element analysis using ICP-MS and ICP-AES Place sample in clean sample bag 5052 DFDP0002 A ShipShore 09-Nov-2011 12:00 Uwe Altenberger Make a thin section and perform SEM and EMPA Impregnate with standard epoxy if too friable to ship intact. Do not heat above 80degC 5052 DFDP0003 A ShipShore 09-Nov-2011 12:00 Edward Dempsey Bob Holdsworth Nic DePaola crush to create a simulated gouge which shall be deformed in a LHVRS testing apparatus to replicate naturally formed gouge from the AFZ Bagged 5052 DFDP0004 A ShipShore 09-Nov-2011 12:00 Roland Oberhänsli Martin Timmermann argon dating of K-feldspar; +/- electron microprobe mineral analysis on polished thin section; polished thin section, electron microprobe mineral analyses, argon dating of micas do not bring in contact with chlorine (Cl)-bearing substances; avoid chlorite-rich parts; do not bring in contact with chlorine (Cl)-bearing substances; 5052 DFDP0005 A ShipShore 09-Nov-2011 12:00 Tetsuro Hirono Make a thin section cut parallel to the mineral liniation and perpendicular to the foliation, minor element and Sr isotope analyses, EBSD analyses, IR analyses; Make a thin section cut parallel to the mineral liniation and perpendicular to the foliation, EBSD analyses, IR analyses Impregnate with standard epoxy if too friable to ship intact. 5052 DFDP0006 A ShipShore 10-Nov-2011 12:00 Elisabettina Mariani Make a thin section and perform TEM, FTIR, XRD DO NOT Impregnate with epoxy. Do not heat above 80degC. 5052 DFDP0007 A ShipShore 09-Nov-2011 12:00 Catriona Menzies Put core in XRF core scanner, Thin Section, pick out chlorite, epidote and calcite for geochemical and isotopic analysis; Pick out the vein minerals for geochemical and isotopic analysis; Analyse for whole rock geochemistry and separate epidotes for geochemical analysis; Pick out the calcite for geochemical analysis etc. No impregnation, wrap in cling flim/ shrink wrap then pad out. 5052 DFDP0008 A ShipShore 06-Nov-2011 12:00 Achim Kopf Matt Ikari intact sample friction, geomechanical properties & experimental microstructure kept intact 5052 DFDP0009 A ShipShore 09-Nov-2011 12:00 Demial Saffer Chris Marone Friction tests (direct shear) on intact wafers and powdered gouge under controlled pore pressure conditions, to measure frictional strength and constitutive properties at low slip rates (0.0001 to 1 mm/s) and normal stresses from 5 to 150 MPa. Sample should be wrapped tightly with shrink wrap (twice) and packed in foam. 5052 DFDP0010 A ShipShore 09-Nov-2011 12:00 Demial Saffer Measure permeability and sonic wave speeds on 1inch plugs under effective stresses from 2 - 100 Mpa. Measurements will be made perpendicular to foliation/fabric (and parallel to it where possible). Sample should be wrapped tightly with shrink wrap (twice) and packed in foam. 5052 DFDP0011 A ShipShore 10-Nov-2011 12:00 Daniel Faulkner Make cores for P & S wave/ permeability/ frictional tests Pack as is 5052 DFDP0012 A ShipShore 11-Nov-2011 12:00 Thomas Mitchell Steven Smith 1) Carry out microstructural (e.g. optical, SEM, microprobe) and mineralogical (e.g. XRD) analyses of natural fault gouges. 2) Carry out friction measurements using low- to high-speed rotary-shear apparatus located in INGV, Rome, and the University of Padova. Both apparatus are equipped with sample holders for use with incohesive (e.g. gouge) materials. More details about apparatus and experimental methodologies are available on request. 3) Compare microstructures of the natural fault gouge with those produced during experiments over a wide range in slip speeds. Gouge block should be kept in a sealed bag for transport. Any loose gouge material should be kept in a sealed plastic bag, and not exposed to direct sunlight for prolonged time periods. 5052 DFDP0013 A ShipShore 11-Nov-2011 12:00 Harold Tobin Make core plug plus possible epoxy impregnate after for sectioning wrap watertight and to maintain cohesion 5052 DFDP0014 A ShipShore 11-Nov-2011 12:00 Geoffrey Batt Thermochron No special handling requirements 5052 DFDP0015 A ShipShore 28-Nov-2011 12:00 Christoph Janssen Impregnate with standard epoxy if too friable to ship intact. Do not heat above 80degC 5052 DFDP0016 A ShipShore 15-Oct-2010 12:00 David Lockner Friction at higher T 5052 DFDP0017 A ShipShore 01-Jan-2012 12:00 Ben van der Pluijm 1 cm cubed blocks (or more if possible) for clay fabric analysis and clay mineraloy. It is important to get samples from within the core so that they have not been contaminated by drilling fluids; modified request from that submitted after talking to Anja Schleiche - to obtain a representative set of samples crossing PSZ-2 in run 69_2 5052 DFDP0018 A ShipShore 07-Oct-2011 12:00 Brett Carpenter 5052 DFDP0019 A ShipShore 15-Oct-2010 12:00 Martin Timmermann 5052 DFDP0020 A ShipShore 15-Oct-2010 12:00 Richard Wing 5052 DFDP0021 A ShipShore 15-Oct-2010 12:00 Hannah Scott 5052 DFDP0022 A Post-Mort 21-Jan-2014 00:00 Ludmila Adam Virginia Toy Electrical and elastic property measurements, and microstructural characterisation 21-Jan-2014 00:00 5052 DFDP0023 A Post-Mort 17-Sep-2015 00:00 Virginia Toy Martina Kirilova Graphitic material for analyses of isotopes to determine source of graphite. 17-Sep-2015 00:00 17-Sep-2015 00:00 5052 DFDP0024 A Post-Mort 11-Nov-2015 00:00 Andrew Greenwood Virginia Toy Possibly for measurements of p wave velocity under load for comparison to Geotek measurements 11-Nov-2015 00:00 5052 DFDP0025 A Post-Mort 07-Mar-2016 00:00 Jack Williams Neutron scanning at Lucas Heights, Sydney, for tomography 07-Mar-2016 00:00 07-Mar-2016 00:00 5052 DFDP0050 A Mort 23-Oct-2014 00:00 Virginia Toy Routine subsamples of cuttings taken onsite for thin sectioning Two subsamples: 1. bulk and 2. quartz-rich 23-Oct-2014 00:00 5052 DFDP5000 A Mort 21-Jan-2015 00:00 Simon Cox Grain size analysis by sieiving 21-Jan-2015 00:00 5052 DFDP5001 A Mort 21-Jan-2015 00:00 Jamie Howarth Phaedra Upton Grain size analysis 21-Jan-2015 00:00 5052 DFDP5002 A Mort 21-Jan-2015 00:00 Simon Cox Carbon14 dating of wood fragments 21-Jan-2015 00:00 5052 DFDP5003 A Mort 21-Jan-2015 00:00 Jamie Howarth Phaedra Upton Carbon14 dating of wood fragments 21-Jan-2015 00:00 5052 DFDP5004 A Mort 22-Jan-2015 00:00 Virginia Toy Reference set of cuttings thin sections for mineralogy (descriptive, by selected point counting, by selected EDS), microstructure (descriptive, selected EBSD?), quartz grain size analysis (linear intercept), FTIR for fluid distribution and content, cataclasite distribution (if present), sequence of structural events, sequence of alteration (CL and EDS mapping) Semple to be submitted to Brent Pooley for thin section manufacture 22-Jan-2015 00:00 5052 DFDP5005 A Mort 22-Jan-2015 00:00 Virginia Toy Elisabettina Mariani Reference set of cuttings thin sections for mineralogy (descriptive, by selected point counting, by selected EDS), microstructure (descriptive, selected EBSD?), quartz grain size analysis (linear intercept), FTIR for fluid distribution and content, cataclasite distribution (if present), sequence of structural events, sequence of alteration (CL and EDS mapping) To be sent to Liverpool for thin sectioning 22-Jan-2015 00:00 5052 DFDP5006 A Mort 22-Jan-2015 00:00 Virginia Toy Timothy Little Reference set of cuttings thin sections for mineralogy (descriptive, by selected point counting, by selected EDS), microstructure (descriptive, selected EBSD?), quartz grain size analysis (linear intercept), FTIR for fluid distribution and content, cataclasite distribution (if present), sequence of structural events, sequence of alteration (CL and EDS mapping) Sample to be sent to Victoria Univ. for thin section manufacture 22-Jan-2015 00:00 5052 DFDP5007 A Mort 22-Jan-2014 00:00 Virginia Toy Norio Shigematsu Reference set of cuttings thin sections for mineralogy (descriptive, by selected point counting, by selected EDS), microstructure (descriptive, selected EBSD?), quartz grain size analysis (linear intercept), FTIR for fluid distribution and content, cataclasite distribution (if present), sequence of structural events, sequence of alteration (CL and EDS mapping) Sample may be sent to Tsukuba for thin section manufacture if Brent Pooley (Otago) cannot get through all submitted sections before end of March 2015. Not yet separated as these are the ones we will try to get quartz separates from: methodology in progres 22-Jan-2014 00:00 5052 DFDP5008 A Mort 22-Jan-2015 00:00 Catriona Menzies Virginia Toy Damon Teagle XRF of cuttings; routine data Send to Catriona Menzies at Southampton. Requires ~30-50g of washed cuttings 05-Mar-2015 00:00 5052 DFDP5009 A Mort 22-Jan-2015 00:00 Carolyn Boulton Elisabettina Mariani XRD of cuttings; routine data Send to Carolyn Boulton at University of Liverpool. Requires ~20g of washed cuttings 05-Mar-2015 00:00 5052 DFDP5010 A Mort 22-Jan-2015 00:00 Anja Schleicher Virginia Toy XRD of cuttings; routine data Send to Anja Schleicher at Potsdam. Requires ~20g of washed cuttings 05-Mar-2015 00:00 5052 DFDP5011 A Mort 22-Jan-2015 00:00 David Lockner High temperature frictional properties measurements Send to David Lockner at USGS Menlo Park. Requires ~500g of unwashed cuttings 05-Mar-2015 00:00 5052 DFDP5012 A Mort 22-Jan-2015 00:00 Catriona Menzies Virginia Toy Damon Teagle XRD of cuttings; routine analysis Send to Catriona Menzies at Southampton; requires ~20g of washed cuttings 05-Mar-2015 00:00 5052 DFDP5013 A Mort 22-Jan-2015 00:00 Lucia Capova Rupert Sutherland Measure its density while gradually increasing its temperature; Changes of density with temperature Shake mud sample bottle then decant ~100ml into another plastic bottle. Send to Lucie Capova at VUW 05-Mar-2015 00:00 5052 DFDP5014 A Mort 28-May-2015 00:00 Loren Mathewson Online Gas Analysis (OLGA) samples. Registered after completion of drilling project. 28-May-2015 00:00 28-May-2015 00:00 5052 DFDP5015 A Mort 29-Jul-2015 00:00 Timothy Little Virginia Toy Systematic thin sections x 2.1. for analysis of modal mineralogy using EDS and quartz grain size using EBS. 2. For study of ductile shear zone kinematics by comparison of LPO and shear band orientations 31-Jul-2015 00:00 5052 DFDP5016 A Mort 28-Jul-2015 00:00 Mai-Linh Doan Douglas Schmitt Sonic velocity, electrical resistivity and porosity measurements Prefer cores, 2cm diameter, as long as possible, parallel and perpendicular to foliation if possible 31-Jul-2015 00:00 5052 DFDP9999 A unknown 15-Oct-2010 12:00 Virginia Toy